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Physisorption represents a powerful methodology, as various structural parameters can be obtained, such as the pore size distribution, surface area (eg, by the BET formalism), and the overall meso- and micropore volume However, although there is no difference in the theory between physisorption in porous bulk materials and thin lms, the standard setups and experimental procedures introduced for the bulk are not applicable to lms As a main problem, physisorption analysis on thin lms has to face the low quantities of material and the fact that the lms are prepared on a substrate, which impedes the analysis for several reasons Standard setups for the characterization of powders, using nitrogen or argon, require at least a surface area of several meters squared, which demands at least ca 10 mg for any valid analysis Evidently, the amount of material in thin lms can be orders of magnitude less.

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Scratching off material from a large number of samples is not desirable because of potential damage to the mesostructure Therefore, signi cant effort has been dedicated in the past years to develop strategies to allow for physisorption experiments on a single specimen of thin lm, ie, typically with a specimen area of the order of 1 cm2 only Three main approaches have emerged to ll the gap of routine physisorption measurements on thin lms 9321 Krypton Sorption Volumetric adsorption using gases with low saturated vapor pressure has been found to be an effective technique to gain detailed structural information for small quantities of porous materials, especially using krypton (Kr)27 The substitution of nitrogen by Kr reduces signi cantly the amount of unadsorbed molecules in the dead volume, allows for the characterization of small surface areas, and is thus ideal for mesoporous.

The enterprise depends on several components on the Internet that are vital to its existence in general. These include DNS, the locator service for the entity on the Internet, and the Internet registration authorities that provide the entity the right (for a fee) to participate in a global Internet infrastructure. These rights include the registration of your domain names and the assignment of IP addresses, without which you are unreachable. Pay attention to the following short list of items as you examine the external environment: How is the company connected to the Internet How does the company use the Internet s DNS system What are the public domains used by the enterprise Who keeps the domains and makes sure that the fees are paid on time Are the domains that you need to register available

(7.21) be the least squares estimate of an arbitrary linear combination If F is normal, then d is automatically normal.

Concentration in the solution (ppb)

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And at low frequencies, Zin 0 r + ( o + 1) Re . (12.103)

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