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Ammonolysis of Nylon 6,6 Ammonolysis is the preferred route currently in use at the DuPont Company for the depolymerization of nylon 6,6 carpet waste [7, 37] McKinney [38] has described the reaction of nylon 6,6 and nylon 6,6/nylon 6 mixtures with ammonia at temperatures between 300 and 350 C and a pressure of about 68 atm in the presence of an ammonium phosphate catalyst to yield a mixture of the following monomeric products: HMDA, adiponitrile, and 5-cyanovaleramide from nylon 6,6 and -caprolactam, 6-aminocapronitrile, and 6-aminocaproamide from nylon 6 The equilibrium is shifted toward products by continuous removal of water formed Most of the monomers may be transformed into HMDA by hydrogenation Kalfas [39] has developed a mechanism for the depolymerization of nylon-6,6 and nylon-6 mixtures by the ammonolysis process.
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The mechanism includes the amide bond breakage and amide end dehydration (nitrilation) reactions, plus the ring addition and ring-opening reactions for cyclic lactams present in nylon 6 On the basis of the proposed mechanism, a kinetic model was developed for the ammonolysis of nylon mixtures Bordrero et al [40] utilized a two-step ami/ammonolysis process to depolymerize nylon 6,6 The rst step is based on an aminolysis treatment of nylon 66 by n-butylamine at a temperature of 300 C and a pressure of 45 atm Free HMDA and N N -dibutyladipamide are generated The second step is ammonolysis of N N -dibutyladipamide at a temperature of 285 C and a pressure of 50 atm The end product is adiponitrile (ADN) It is estimated that the yields could be about 48% for ADN and about 100% for HMDA at optimized reaction conditions.
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Recovery of Nylon 6,6 Monomers Adipic acid and HMDA are obtained from nylon 6,6 by the hydrolysis of the polymer in concentrated sulfuric acid (Fig 163) The adipic acid is puri ed by recrystallization, and the HMDA is recovered by distillation after neutralizing the acid This process is inef cient for treating large amounts of waste because of the required recrystallization of adipic acid after repeated batch hydrolyses of nylon 6,6 waste In a continuous process [25], nylon 6,6 waste is hydrolyzed with an aqueous mineral acid of 30 70% concentration and the resulting hydrolysate is fed to a crystallization zone The adipic acid crystallizes and the crystals are continuously removed from the hydrolysate Calcium hydroxide is added to neutralize the mother liquor and liberate the HMDA for subsequent distillation Continuous recovery requires adipic acid crystals having an average diameter of ca 40 50 nm.
Ingredients Other Than Elastomers Used to Compound Rubbers for Pharmaceutical Industry Pigments Carbon black Titanium dioxide Iron oxide Barium sulfate Zinc oxide Silica Chromium oxide Organic dyes
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